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1.
The Er3+ doped oxyfluorogermanate glasses, with a composition containing Na element, were synthesized by the conventional melting–quenching technique. When Na element was introduced into the composition of oxyfluorogermanate glass, the crystals behavior was investigated in details. Depending on the annealing procedure supplied, thermal annealing of precursor glasses in the system GeO2/BaF2/AlF3/Na2O/NaF/ZnO/GdF3/ErF3 led to the precipitation of different crystal phase nanocrystals. It was confirmed the nanocrystals in GC600 is orthorhombic NaBaAlF6 which led to enhance obviously in the UC luminescence of Er3+. However, the nanocrystals in G585 led to decrease in the UC luminescence, which indicated few Er ions enter into the lattice of this nanocrystal phase. The reason of the decrease in UC emission intensity of GC585 was analyzed. 相似文献
2.
Wenhui MA Gang XIE Hua WANGFaculty of Materials Metallurgical Engineering Kunming University of Science Technology Kunming China Manuscript received January in revised form May 《材料科学技术学报》2002,18(3):286-287
The thermal expansion behavior of La1-xSrxMn1-yCoyO3-δ (x=0.2-0.4, y=0.1-0.3) perovskites in air has been investigated. The average linear thermal expansion coefficients increased with increasing Sr content up to 40 mole fraction or Co content up to 30 mole fraction. The expansion is generally attributed to an increase in the average cation radius as some of the cations in the perovskite are reduced in valence when oxygen ions are removed from the structure. 相似文献
3.
YAG:Ce Phosphors for WLED via Nano-Pesudoboehmite Sol-Gel Route 总被引:5,自引:0,他引:5
The sub-micron sized YAG : Ce phosphors were synthesized via a modified sol-gel method by peptizing nano-pesudoboehmite particulate. It is found that YAG phase from the dried gel powders appears at 1000 ℃ then the pure YAG phase exists at a relatively lower sintering temperature of 1400 ℃. The smaller sizes of phosphors in the ranges of 1 - 3 μm are obtained due to the contribution of seeding effects of nano-sized alumina particles to strengthen each step of the processes. Both the excitation and emission spectra of photoluminescence of the phosphor obtained at 1400 ℃ meet well with the spectroscopic requirements of the WLED phosphors. 相似文献
4.
《Biomass & bioenergy》2006,30(8-9):803-808
The papermaking properties of 22 pure and hybrid poplars are being evaluated in an on-going investigation. Twenty of the poplars were harvested after 7.5 years from three different sites in the Midwestern and North Central US. The other 2 poplars survived at only two of three sites (64 total samples). The Crandon hybrid had the highest growth rate (t ha−1 y−1) and wood density (both averaged across the 3 sites). This poplar had a high cellulose content (compared to the average), a low lignin content and produced bleached kraft fibers at a high yield (wt.% on wood chips). Further, this poplar responded very well to kraft pulping and oxygen delignification and bleached to the highest final brightness ever observed in our laboratory (94.5% Elrepho). It also produced an 18 kappa number unbleached pulp with <0.5% rejects in only two-thirds the time required for sugar maple (Acer saccharum).We also report on clone 220-5 that had the highest area-weighted average microfibril angle. Pulps from this poplar had excellent tensile properties and further improvements are expected with 1–2 years of additional growth that should result in a small, but significant increase in average fiber length. Some results are also presented for clone 313.55 and aspen (Populus tremuloides) to demonstrate the many substantial benefits that can be accrued from proper wood selection. 相似文献
5.
《Intermetallics》2006,14(1):75-81
A novel technique has been developed to produce Fe–Al intermetallic coatings on steel. This technique applies mechanical vibration to a retort, which is loaded with Al powder, alumina filler, ammonium chloride activator and FeCrAl alloy balls. The operation temperature was from 440 to 600 °C. This technique produced coatings with thickness of 17 μm for 15 min and 90 μm for 120 min treatment at 560 °C. The coatings appear to be homogeneous, with a high density and free of porosity, and have excellent adherence to the substrate. The coatings consisted mainly of η-Fe2Al5 with small amounts of θ-FeAl3 and β-FeAl, and exhibited a nano-structure. Microstructure studies suggested that the formation of the intermetallic phases at a low temperature has a complex mechanism, including the formation of a thin Al layer on the substrate by ball milling; Al-rich phases nucleation, growth and formation of an initial alloy layer; severe plastic deformation which increases the local temperature and produces a nano-structure; and fast outward diffusion of Fe and formation of Fe–Al intermetallics. This technique reduced the treatment temperature and duration significantly compared with the conventional Al pack cementation processes, providing a new approach to industrial diffusion coatings with great energy and time savings. 相似文献
6.
采用溶胶-凝胶工艺在普通载玻片上制备出C轴择优取向的ZnO:Al透明导电薄膜。利用扫描电镜(SEM)、X射线衍射仪(XRD)等分析手段对薄膜进行了表征。通过标准四探针法及紫外分光光度计(UVS)透射光谱研究了ZnO:Al薄膜的电学与光学性能。实验发现:当Al^3+离子掺杂浓度为2%(原子分数),前处理温度为220℃、退火温度为580℃时,薄膜具有较好的导电性,电阻率为1.76×10^-3Ω-cm,其在可见光的平均透射率在80%左右。 相似文献
7.
8.
用共沉淀法合成了BaTiO3,研究了Ba1-xNdxTiO3系Nd3+施主一次掺杂在x=0.03~0.065之间时,BaTiO3基陶瓷电容器的本征电性能。结果表明,在此含量范围掺杂的情况下,陶瓷呈绝缘性,Nd3+含量在0.03~0.055左右时随着Nd3+含量的增加,陶瓷的ε增加,Tc呈下降趋势,tgδ值下降。Zr4+的加入也可使材料的ε增加,Tc下降。Mn2+的加入对材料的本征电性能影响不大。Ba1-3x/2NdxTiO3配比比Ba1-xNdxTiO3配比的材料的温度特性要好。 相似文献
9.
《Computer Speech and Language》2014,28(5):1066-1082
In this paper, we describe several approaches to language-independent spoken term detection and compare their performance on a common task, namely “Spoken Web Search”. The goal of this part of the MediaEval initiative is to perform low-resource language-independent audio search using audio as input. The data was taken from “spoken web” material collected over mobile phone connections by IBM India as well as from the LWAZI corpus of African languages. As part of the 2011 and 2012 MediaEval benchmark campaigns, a number of diverse systems were implemented by independent teams, and submitted to the “Spoken Web Search” task. This paper presents the 2011 and 2012 results, and compares the relative merits and weaknesses of approaches developed by participants, providing analysis and directions for future research, in order to improve voice access to spoken information in low resource settings. 相似文献
10.